Fritsch Analysette 22 NeXT droog dispergeereenheid

ANALYSETTE 22 NeXT DRY DISPERSION UNIT

The sample material is transported with a vibratory feeder through the intake funnel into the dry measuring cell, where it falls directly into a Venturi nozzle operating with an adjustable flow of compressed air. Upon passing through the nozzle, agglomerates are broken up and the measurement of the particle size dispersion in the laser beam takes place directly afterwards. For dry dispersion the required sample volume is 1 – 300 cm3, which is larger compared to wet dispersion; however it is also easier to obtain a representative analysis.

• Fast measurement of powdery samples in an accelerated airflow
• For sample volumes from less than 1 cm3 to approx. 300 cm3
• Efficient degradation of agglomerates with a special
• Venturi nozzle
• No impact areas – protection against comminution of the particles
• Perfect sample feeding with high frequency feeder
• Automatic computer-controlled adjustment of the dispersion pressure
• Fully automatic, freely programmable measurement processes
• Especially fast and easy to clean - without tools

The sample material is feeded through the height-adjustable funnel and stirrer onto the high-frequency feeder and continuously transported over the funnel-shaped opening of the dry measuring cell and then drops in the actual dispersion area. In a Venturi nozzle the powder is accelerated and passes with a high speed through the nozzle channel and the measurement of the particle size distribution in the laser beam takes place directly behind it. Then it passes a zone with aerodynamic wave generation at the nozzle outlet. The by the high turbulent current caused strong shearing forces, as well as blows between the particles lead to the breakdown of the agglomerates. No impact areas in the flight path of the particles exist in order to prevent soft sample materials from being ground during the dispersion process.

Compared with the wet dispersion is the dry dispersion not as efficient due to chemically-physical as well as rheological material properties of the sample material.

One of the main differences between dry and wet dispersion is based on the fact, that it is almost a solely mechanical dispersion in an air flow. Thereby, with a dry dispersion, a sensible measurable particle size and the associated complete primary particle dispersion is typically at approximately 1 - 10 µm. Depending on the material and its properties, below this range an incomplete dispersion can be expected. The utilization of the dry dispersion makes sense in areas where a wet dispersion in water or solvents has to be ruled out.

For the operation of the dry dispersion unit, an oil-, water- and particle-free supply of compressed air with a pressure of at least 5 bar and an air volume of at least 125 l/min is required. An external exhaust system is necessary to vacuum the sample material and can be ordered as a FRITSCH accessory together with the instrument.